This is just an introduction
to help take the 'mystery' out of the big, thirteen
dollar words you see concerning heat treating of
steel. It'll also establish the steps you need to
take before the actual quenching operation.
I'll keep it basic and
understandable, but it's important that you know
what's actually going on inside the piece of steel
you're working with. And also, that you know the
most important terms so you'll know what you're reading
when you look at books on the subject.
The steel I'll use for
this intro is plain, low alloy carbon steel; 1084.
There are many reasons why this is a good steel to
use for forging blades and it brings up the first
funky word: Eutechtoid. The big heads in metallurgy
say that the Euthchtoid, or the balance point for
carbon/iron content in steel is .85% or 85 points
of carbon. All that means to me and you is that there's
not much of a reason to use steel with more carbon
than that for knife blades unless you're dealing
with high alloy, high carbon steels. Higher carbon
content would be referred to as 'hyper-eutechtoid'.
Lower carbon content would be referred to as 'hypo-eutechtoid'.
Enough about that.
If you don't get anything
else out of this tutorial, get this. Don't trust
your eyes to determine when the steel is ready to
normalize, anneal, or quench. You just won't get
good, consistent results. (Ask me how I know). Use
a magnet to determine when the steel is at a nonmagnetic
state.
Now, it's important that
you know that steel behaves differently with a magnet
during the heating/cooling process. When you're heating
your blade up in the forge, the steel will get progressively
hotter and change colors continuously starting from
the first hint of dull red all the way through the
spectrum. ON THE WAY UP, your magnet will not lie
to you. On the way down however, the steel will remain
nonmagnetic for a long period of time. I kind of
started in the middle there, but you'll see why in
a minute.
When you start out with
a piece of steel, it's in the 'Alpha' state or at
room temperature. As you heat it up, it will change
structure to 'Gamma' at the critical temp or nonmagnetic
Gamma simply refers to the changed state of the steel
known as 'Austenite'. The point at which the steel
becomes Austenite is very important. Several things
happen at this stage. I know you've all seen what's
referred to as the shadow in hot steel. Well, that
shadow is the dividing line between the Austenite
or Gamma structure (higher temp) of the steel and
the Alpha structure (lower temp) of the steel. So,
as the steel heats up, the shadow moves through the
steel from the higher temp area toward the low temp
area or from the end of the bar/blade towards the
handle. (Scratching my head here, how to get the
point across?)
This shadow is your visual
cue that you need to check with the magnet. So, when
you see the shadow in the steel as you're heating
it up, start checking it with the magnet for critical
temp in the steel. In the completely forged blade,
the shadow will travel up from the edge toward the
spine. From the thinner to thicker sections of the
blade. It will follow any curves in your blade as
well. Pay close attention the next time you're heating
up a finished blade and you'll see what I mean. Don't
get it too hot and then wait for the magnet test
to work because it won't work on the way back down.
I can't stress this point enough. If you get the
steel too hot it will cause grain growth and you'll
have to stop and normalize the steel in order to
get this under control. That brings up normalizing.
Normalizing is the slow,
even heating and cooling of the steel to get all
the carbon and iron in a stress free state and ready
for annealing. This is done after forging the blade
to shape. To do this, simply heat the steel evenly
to nonmagnetic and let it air cool down to a black
heat or where all 'visible' color has left the steel.
Lay the blade spine down to avoid overheating the
edge. Do this three times. I usually just heat up
the steel and then walk around the smithy with the
bar till it's at a black heat and then repeat the
process.
If you're going to anneal
the steel, you do this on the third normalizing sequence.
So, instead of heating it up and letting it cool
in the air, heat it up and put it in ashes or vermiculite
or what have you. In order to anneal properly, don't
leave any steel exposed from the ashes. Hot cut your
blade off of the bar you're forging from before annealing
it so it can be totally covered with ashes during
annealing. If you're using tongs, you won't need
to hot cut anything as long as the entire blade will
fit in the annealing bucket. This slow cooling should
take 8 - 12 hours. Don't be impatient and pull it
out to check on it. That will only undermine an otherwise
great anneal. Now is the time to start on another
forging project or work on other knives.
I've had the best luck
with fine hardwood ashes. The only bad thing about
this is that the ashes will melt onto your blade
and make a mess. Just soak it in white vinegar overnight
and it comes off clean as a whistle. If you don't
want to wait, just heat the vinegar to below boiling
and put the blade in that. It will clean up pretty
fast. Save the vinegar for this and it will get stronger
and faster each time as the water is boiled out of
it.
Why anneal at this point?
Well, I'm assuming that we just normalized a fully
forged blade, ready for hand working. I always anneal
at this point because I want the steel at it's softest
so it's easier to file, stamp and so on.
Now, I mentioned grain
growth earlier and I'll explain it now. When you
get the steel too hot during forging, the grain gradually
gets larger and larger. It's most critical at the
normalizing, annealing and heat treating phase. So,
all the heating/cooling, heating/cooling that went
on during the forging process has the steel in a
very uneven state and it most likely is stressed
from cooling unevenly on the anvil and from hammer
blows, etc... I don't know exactly why the grain
grows, it just does. And it will kill an otherwise
good blade deader than a door nail. To avoid grain
growth, use the magnet in all phases of normalizing,
annealing and quenching! It's that simple.
If you do everything else
right all the way up to the quench and then overheat
the steel for quenching, all that work was for nothing
and you have to start over with the normalizing process.
The grain size will be large and sandy looking if
you break the blade at this point. It will still
get hard, but it won't hold an edge and the steel
will be weak. That's what happened to my test blade
in the intro class. I did everything else right all
the way up to the quench and overheated the steel
before quenching. When the blade broke in the vise,
it had large grain. DUH! I didn't use a magnet. I
resisted that little trick until then. I guess a
hard head like me just has to learn the hard way.
That's all it took. Seeing is believing and now I'm
a firm believer in the magnet trick.
So, to recap this part
of heat treating - USE THE MAGNET! It's just that
simple. There are probably some of you guys out there
that are saying 'Oh, BS, I can judge the color of
the steel'. You're probably right. Experience is
the key to your success. But, for the majority of
us blade bangers, the magnet is the key.
In the next part, I'll
go over some more thirteen dollars words and get
to the meat of the matter - What happens when you
quench the blade and how to get the most out of your
techniques. Thanks for looking in on me and please
ask all the questions you can think of. I know I'm
a little disjointed with my presentation, but I think
I got all of my points across to get you primed for
the next part of heat treating.
Oh, thanks Ron. I was thinking
about it, I just forgot to write it down clearly. If
you get grain growth from overheating your steel, it's
a simple matter to 'normalize' the grain structure again
by normalizing it. Up to a certain point, anyway. If
you really overheat your steel several times, there is
a point of no return with the carbon in the steel. Burn
your steel just once and your total carbon content in
the burned section is reduced. I've been told that if
you burn a piece, even slightly, just cut it off and
start over. I don't believe you can do anything to restore
the carbon or reduce the grain size at that point. How
do you reduce the grain size and keep it there? Quench
the properly normalized blade at nonmagnetic!
So,
you've done whatever grinding, filing, stamping
and sanding you intend
to do on the blade. By the way, how fine a finish
should you take your blade to before the quench?
There are lots of opinions about it. I used to get
silly and forget that my blade wasn't ready for final
finishing just about the time I finished it. Hmmm.....
If you're quenching in oil, there's not much reason
to go any finer than 220 grit prior to the quench.
You want to get all the surface irregularities out
of the steel before the quench. If you don't there's
a good possibility that you can get heat risers or
stress risers that will crack and ruin all your hard
work. After the quench, you'll want to grind off
at least a little of the surface, especially on the
edge because of decarburization. That's why it's
important to leave the edge thick for the quench.
So you can get down into the hardened steel and have
a good, high carbon edge on the finished blade. Also,
it's a good idea to wait until after the heat treating
is finished to grind your ricasso shoulders on a
hidden tang blade. If you file the shoulders to a
sharp 90 degree angle, it might crack during the
quench. You'll have to draw the tang and ricasso
back in order to do that. Just suspend the blade
in a pan of water and heat the ricasso and tang to
a purple heat and let it cool. It's best to radius
the shoulders anyway. If you radius the shoulders,
it won't make any difference when you quench.
In the past, when I forged
a tribal piece I left the surface 'as forged' and
just cleaned the scale off by soaking it in vinegar
overnight. Then, I'd do some hand sanding to highlight
the texture and make it look good (to me anyway).
Now however, I take the surface of the blade to a
fully finished, flat surface to avoid the cracking
and warping that can occur on an irregular blade
surface with hammer dings and scale pitting during
quenching. I still forge tribal blades, I just take
a lot more time during the finishing heats to flatten
the blade surface as close to finished as possible
for minimal cleanup. Keeping the face of your anvil
clean will help tremendously with that process.
Now, I'm not saying that
tribal, 'as forged' pieces are necessarily going
to fail. It's just a lot more likely that they will
given the nature of most of the steels we work with.
Take 5160, for example. I was working with a piece
of 5160 yesterday that I brought home from school.
They let us have the short scraps to bring home and
play with. Well, that particular batch of 5160 was
full of inclusions, or tiny cracks from the manufacturing
process. You won't know those cracks are there unless
you clean up the surface down to bare, shiny metal.
That's the point I'm trying to make here. You won't
know the cracks are there unless you can see them.
So, when it's an important blade, finish it accordingly
for the best quality.
So, we have a blade that's
been normalized, annealed and otherwise finished
up ready for the quench. There are several ways to
heat the blade up for the quench. You can use the
coal or gas forge, an oxy/acetylene torch, an electric
heat treat oven or whatever will allow you to heat
the steel slowly and evenly to a uniform critical
or nonmagnetic heat. There are several quenching
methods as well. We're quenching a blade forged from
1084, so we'll use oil.
There's a lot of controversy
over which oil to use. I learned so much about different
quenching mediums at school that it got kind of confusing
at times. Here are some key elements to think about
when you're selecting your quenching oil. First and
foremost, choose a light oil with a high flash point.
Some folks say to use organic oils like vegetable
oil, linseed oil, transmission fluid, bear grease....
the list goes on and on. I think the vast majority
of us use old motor oil. That's what I've used for
years because it's what I learned to use. It's not
the best, but it works. I'm still using it because
that's what I have. I do intend to get myself some
Chevron quench oil, I just haven't done it yet. The
oil you use isn't nearly as important as your technique.
Probably the most important
thing to do with whatever oil you're using is to
preheat it before the quench. I never preheated my
oil in the past because it didn't seem important
with my limited knowledge. It's very important! You
should always preheat your oil to around 150 F. A
good way to do it is to heat up a big hunk of junk
steel and quench it until the oil is at a temp that
is 'almost' uncomfortable to put your finger in.
You can use a candy thermometer if your wife don't
find it out
The reason it's important
to preheat your oil is because of the vapor barrier
that forms around the steel immediately at the time
of quenching. It really has very little to do with
the temp of the oil. Actually, it has more to do
with the viscosity or thinness of the oil. When you
heat the oil up, it gets thinner. That means less
of a vapor barrier around the steel when you quench.
Lets look at that vapor barrier a little closer.
When you quench a blade,
very little oil actually contacts the surface of
the steel initially because the oil vaporizes on
the surface and puts a vapor jacket or barrier around
the steel. Now, this all happens pretty fast and
is usually accompanied by a flame that jumps up and
catches your beard on fire and blinds you with thick,
white smoke. As the steel cools down to below the
flash point of the oil, the oil finally comes into
contact with the steel and cools it down quickly.
But, right at first, the oil is doing very little
cooling to the steel. It's the oil vapor that's cooling
it. You can begin to see that it's not as simple
as you once thought it was. It's really quite complicated
and bears considerable thought to really understand
what's going on in your quench tank.
Water is even worse. Most
oils have a flash or boiling point of around 450
F. Water doesn't have a flash point, but it boils
at 212 F at sea level. So, the steel has to get down
to 212 F before the water actually comes into contact
with the steel. All the way from 1550 F to 212 F,
the steel is surrounded by a vapor barrier. The water
is actually boiling just off the surface of the steel!
That makes for a very poor quench medium.
Time for some more thirteen
dollar words. A bunch of 'ites'. We talked about
Austenite yesterday. That's the gamma state of the
steel during the heating up process. Austenite is
the beginning of the transformation of the steel
into a useable blade. When the steel has been transformed
into austenite at the nonmagnetic target temp, it's
time to quench. Now, 1084 steel is considered a very
fast quenching steel. In other words, you have approximately
3/4 of a second to get the temp down from nonmagnetic
to around 400 F in order to get the best conversion
to Martensite, which is most desirable form of steel
to the knifemaker. Martensite is very crystalline
in structure. It looks like a bunch of needles in
a pile going every which a way. Martensite gives
steel its hardness. But, it's very unstable and is
under a tremendous amount of stress. Because, what
you've just done is cause the steel to be in a state
that it doesn't want to be in. You tricked it by
freezing it's structure at a determined point.
Now, if you don't have
the right oil, or it's not preheated correctly, the
quench won't be rapid enough and you will most likely
transform the steel into Pearlite. Pearlite is still
fairly hard, but it's not as fine or hard as Martensite.
This gets very confusing, but try and stay with me.
There is coarse Pearlite and fine Pearlite. If you
miss the quench time by a second or two, you will
most likely get fine Pearlite. If you miss it by
more than a few seconds, you'll most likely get coarse
Pearlite. Fine Pearlite is acceptable, but coarse
Pearlite is bad news.
So, a rapid quench is necessary to produce Martensite, which is what you want
in your blade.
Now lets look at a few
quenching techniques. Edge quenching is very popular
and I use it myself. There are a few ways to do it.
First, you can just heat up the edge to nonmagnetic
and quench the entire blade edge down until the oil
stops bubbling. That's pretty tricky to get right.
You have to be very precise with your heat so you
don't overheat the edge and especially the point.
Then, you have to be extremely fast on the quench
because the edge won't hold the temp for long. The
other way to edge quench is to heat the entire blade
up all the way into the ricasso and then quench edge
down for at least 1/3 the width of the blade. Rock
it back and forth along the edge until all the color
leaves the spine. Then, dip the blade in the oil
until it's cool enough to handle. If you take it
out of the oil, the heat in the spine may draw the
hardness out of your edge. Some folks use a brick
or hunk of steel to set the quench depth in the oil.
I just use the edge of the pan as a guide. It works
for me.
The full quench is easier,
but can cause warping if not done correctly. Heat
the entire blade to nonmagnetic and quench the entire
blade edge first. Just put it straight into the oil
and leave it there. Don't move it around until the
most violent bubbling and gurgling is gone. This
is a good time to bring up Mar-Quenching or 'Quenchus
Interuptus' as Kevin Cashen likes to call it. It's
a new technique he's developed that makes a lot of
sense to me. After the oil stops bubbling and smoking,
take the blade out and look at it quickly. If the
oil is smoking, but not burning off, you're at right
around 450 F. This is where you interrupt the quench.
Leave the blade out of the oil and let it cool to
room temp. According to Kevin, this will result in
a better transformation to Martensite.
I had been doing that
in a different way. It just seemed to make sense
to me. I would quench the blade until it quit burning
the oil, then put it in the ashes until it cooled.
What I was trying to do was shortcut the tempering
process which I'll cover next. I told Kevin about
what I had been doing and he wasn't sure that was
a good thing or necessarily a bad thing. The jury
is still out on it for now.
Anyway, after the blade
is cool enough to handle, clean off the oil residue
with a scotch brite pad or sandpaper so you can see
the tempering colors later on. Actually, the easiest
way to get the oil crud off is to use a scotch brite
pad as soon as you remove it from the oil. It will
come right off when the blade is still hot.
Now, place the blade immediately
in your tempering oven. Don't delay the tempering
of your blade. If left even for a few hours, it could
begin to crack as the Martensite starts to form.
Martensite expands as it forms which is why the blade
cracks if not tempered right away. I use a toaster
oven because they have a smaller variation of temperature
in most cases. A kitchen oven can fluctuate as much
as 100 F during the tempering process. That's not
good for the tempering process. Use whatever you
have available that will maintain a nice, even temp.
For 1084, 400 F is about right for a good hard blade
that's tough as well. I don't know the Rockwell scales,
but if I remember right 400 F for one hour will give
you somewhere in the neighborhood of 56 - 59 RC.
Some folks do a triple temper. I haven't tried it
yet but intend to. The main thing to remember with
tempering is that you're taking the stress out of
the steel and allowing the Martensite to finish forming
in a stable environment. No sudden temperature changes
during tempering. If you triple temper, let the blade
cool down all the way to room temp before you put
it back in the oven. The tempering color I mentioned
earlier is a light straw color. If you cleaned the
blade well enough you should be able to see it before
you take it out of the oven.
Now, for the full quenched
blade, you may want to draw the spine to make it
more flexible and less likely to break during hard
use. That's especially important on a large blade.
Just hold the blade by the tang and lay the edge
in a pan of water and gently heat up the spine to
a nice blue color down to the water line. Be very
careful not to overheat the spine or it will make
the knife weak. Draw the spine three times being
careful not to quench the blade. Let it cool slowly
with the edge in the water.
Finish up your blade and
there you go. Probably the most important thing to
remember when heat treating your blade is being careful
with temperature variations. The only violent temperature
shift you want is with the quench. Be patient, take
your time and you should wind up with a nice, sharp,
tough blade.
.